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1

Rapid hydrophilic interaction chromatography determination of lysine in pharmaceutical preparations with fluorescence detection after postcolumn derivatization with o-phtaldialdehyde

Michal Douša, Jiří Břicháč, Petr Gibala, Petr Lehnert

Journal:

Journal of Pharmaceutical and Biomedical Analysis

Year:

2011

Language:

english

File:

PDF, 291 KB

english, 2011

2

Identification, preparation and UHPLC determination of process-related impurity in zolmitriptan

Michal Douša, Petr Gibala, Stanislav Rádl, Ondřej Klecán, Zuzana Mandelová, Jiří Břicháč, Tomáš Pekárek

Journal:

Journal of Pharmaceutical and Biomedical Analysis

Year:

2012

Language:

english

File:

PDF, 171 KB

english, 2012

3

HPLC Determination of Nitrated Polycyclic Aromatic Hydrocarbons after Their Reduction to Amino Derivatives

Brichac, Jiri, Zima, Jiri, Barek, Jiri

Journal:

Analytical Letters

Year:

2004

Language:

english

File:

PDF, 173 KB

english, 2004

4

Direct and indirect high-performance liquid chromatography enantioseparation of trans-4-hydroxy-2-nonenoic acid

Jiri Brichac, Ales Honzatko, Matthew J. Picklo

Journal:

Journal of Chromatography A

Year:

2007

Language:

english

File:

PDF, 214 KB

english, 2007

5

Enantioselective metabolism of trans-4-hydroxy-2-nonenal by brain mitochondria

Ales Honzatko, Jiri Brichac, Tonya C. Murphy, Alexander Reberg, Alena Kubátová, Irina P. Smoliakova, Matthew J. Picklo Sr.

Journal:

Free Radical Biology and Medicine

Year:

2005

Language:

english

File:

PDF, 500 KB

english, 2005

6

A novel approach for HPLC determination of 2-cynaoacetamide using derivatization procedure with 2-hydroxyacetophenone as a new useful derivatization reagent

Douša, Michal, Břicháč, Jiří, Tkadlecová, Marcela, Man, Stanislav, Zezula, Josef, Hájíček, Josef, Pekárek, Tomáš

Journal:

Journal of Pharmaceutical and Biomedical Analysis

Year:

2016

Language:

english

File:

PDF, 969 KB

english, 2016

7

Esterification of Ibuprofen in Soft Gelatin Capsules Formulations—Identification, Synthesis and Liquid Chromatography Separation of the Degradation Products

Douša, Michal, Meca, Luděk, Gibala, Petr, Jirman, Josef, Tkadlecová, Marcela, Srbek, Jan, Šalandová, Jana, Kovalčíková, Eva, Břicháč, Jiří

Journal:

Journal of Chromatographic Science

Year:

2017

Language:

english

File:

PDF, 508 KB

english, 2017

8

Synthesis of 2-(4-Isopropylthiazol-2-yl)-7-methoxy-8-methylquinolin-4-ol; A Quinoline Building Block for Simeprevir Synthesis

Rádl, Stanislav, Rezková, Hana, Obadalová, Iva, Srbek, Jan, Břicháč, Jiří, Pekárek, Tomáš

Journal:

Year:

2014

Language:

english

File:

PDF, 237 KB

english, 2014

9

ChemInform Abstract: Synthesis of 2-(4-Isopropylthiazol-2-yl)-7-methoxy-8-methylquinolin-4-ol; a Quinoline Building Block for Simeprevir Synthesis.

Radl, Stanislav, Rezkova, Hana, Obadalova, Iva, Srbek, Jan, Brichac, Jiri, Pekarek, Tomas

Journal:

Year:

2014

File:

PDF, 15 KB

2014

10

Direct analysis in real time – High resolution mass spectrometry as a valuable tool for the pharmaceutical drug development

Srbek, Jan, Klejdus, Bořivoj, Douša, Michal, Břicháč, Jiří, Stasiak, Pawel, Reitmajer, Josef, Nováková, Lucie

Journal:

Year:

2014

Language:

english

File:

PDF, 2.80 MB

english, 2014

11

Enantioselective Oxidation of trans -4-Hydroxy-2-Nonenal Is Aldehyde Dehydrogenase Isozyme and Mg 2+ Dependent

Brichac, Jiri, Ho, Kwok Ki, Honzatko, Ales, Wang, Rongying, Lu, Xiaoning, Weiner, Henry, Picklo, Matthew J.

Journal:

Chemical Research in Toxicology

Year:

2007

Language:

english

File:

PDF, 376 KB

english, 2007

12

The formation of furfural compounds in selected saccharide- and polysaccharide-based pharmaceutical excipients

Michal Douša, Petr Gibala, Jiří Břicháč, Jaroslav Havlíček

Journal:

Journal of Pharmaceutical Sciences

Year:

2012

Language:

english

File:

PDF, 291 KB

english, 2012

13

Rapid HILIC method with fluorescence detection using derivatization reaction utilizing o-phthaldialdehyde for determination of degradation product of aliskiren

Michal Douša, Jiří Břicháč, Jiří Svoboda, Robert Klvaňa

Journal:

Journal of Pharmaceutical and Biomedical Analysis

Year:

2012

Language:

english

File:

PDF, 515 KB

english, 2012

14

Drug-excipient compatibility testing—Identification and characterization of degradation products of phenylephrine in several pharmaceutical formulations against the common cold

Michal Douša, Petr Gibala, Jaroslav Havlíček, Lukáš Plaček, Marcela Tkadlecová, Jiří Břicháč

Journal:

Journal of Pharmaceutical and Biomedical Analysis

Year:

2011

Language:

english

File:

PDF, 585 KB

english, 2011

15

Analysis of HNE metabolism in CNS models

Kubatova, Alena, Honzatko, Ales, Brichac, Jiri, Long, Eric, Picklo, Matthew J.

Journal:

Year:

2007

Language:

english

File:

PDF, 110 KB

english, 2007

16

Novel microbial epoxide hydrolases for biohydrolysis of glycidyl derivatives

Michael Kotik, Jiri Brichac, Pavel Kyslík

Journal:

Journal of Biotechnology

Year:

2005

Language:

english

File:

PDF, 164 KB

english, 2005

17

Identification and structure elucidation of a new degradation impurity in the multi-component tablets of amlodipine besylate

Gibala, Petr, Douša, Michal, Kalužíková, Aneta, Tkadlecová, Marcela, Štefko, Martin, Kalášek, Stanislav, Břicháč, Jiří

Journal:

Journal of Pharmaceutical and Biomedical Analysis

Year:

2018

Language:

english

File:

PDF, 770 KB

english, 2018

18

Quantification of trans-4-hydroxy-2-nonenal enantiomers and metabolites by LC–ESI-MS/MS

Ales Honzatko, Jiri Brichac, Matthew J. Picklo

Journal:

Journal of Chromatography B

Year:

2007

Language:

english

File:

PDF, 195 KB

english, 2007

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